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[0022] In some particular embodiments of the present invention, the cleaving in step 2 of the preparation method is performed with an reagent, comprising one or a mixture of two or more of TFA, PhSMe, PhOMe, EDT, H 2 O, TIS or PhOH
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5101533851.8 Retatrutide 24 (least-squares mean percentage change) 1mg 7.24mg 12.98mg 17.3 12mg 17.5
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